AP20187_LCMS_16775_MedChemExpress

File ..0150702 2015-07-02 09-26-01\ZDM2765-001-2.D Tgt Mass (CHM): Injection Date : 2 Jul 15 9:36 am +0800 Seq. Line : 3 Sample Name : ZDM2765-001-2 Location : P1-A-03 Acq. Operator : Li Shan(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 7 ul

Acq. Method : D:\Aglient 1260\Data\20150702\20150702 2015-07-02 09-26-01\100-1500MS+7MIN_ Analysis Method : D:\AGLIENT 1260\METHOD\100-1500MS+7MIN_1.5(0.02%FA).M Catalog No : HY-13992 Batch#16775

Method Info : Postive,MS:100-1000,Column ID:A-RP-85,50℃

min

1

2345

67mAU

500100015002000 DAD1 B, Sig=214,4 Ref=off

2.566

3.973

4.959

5.216

min

12

345

67mAU

50

100

DAD1 C, Sig=254,4 Ref=off A r e a : 27.

9426

A r e a : 2.

43629 A r

e a : 4637.75

2.5644.8875.207min

12

345670

100000

200000

300000

400000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 50

2.561

3.872

4.964

5.106

min

12

34567-0.1

-0.05

00.05 Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.7 Integration Results for DAD1 B, Sig=214,4 Ref=off

RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 2.57 0.13 64.30 8.38 0.06 3.97 0.11 48.03 7.37 0.05 4.96 0.09 51.29 9.63 0.05 5.22 0.66 104354.09 2651.05 99.84

Integration Results for DAD1 C, Sig=254,4 Ref=off

RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 2.56 0.11 27.94 4.30 0.60 4.89 0.09 2.44 0.47 0.05 5.21 0.50 4637.75 154.18 99.35

MS Report

Ret. Time: 2.56 <<<< POSITIVE SPECTRA >>>>

m/z

500

1000

2000

4000

6000

8000

10000 ES-API Positive

225.1 109.9

102.1

213.1

212.1

Ret. Time: 3.87

m/z

500

1000

5000

10000

15000

20000

ES-API Positive

366.1

102.1

259.1

258.1

Ret. Time: 4.96

m/z

25050075010000

2000

4000

60008000100001200014000 ES-API Positive

225.1

318.3

274.3 110.1

416.1

708.3

472.1

395.3

394.1

Ret. Time: 5.11

m/z

50010000

5000

10000

15000

20000250003000035000 ES-API Positive

559.3

404.2

472.1

1119.4

1484.7 1118.5 1482.7

1117.6

366.2

742.1

MS Report